Klaus Eichele:
|
Contents | [2002] [2001] [2000] [1999] [1997] [1996] [1995] [1994] [1993] [1992] [1991] [1990] |
--- 2002 --- | [UP] |
K. Eichele, R. E. Wasylishen, J. F. Corrigan, N. J. Taylor, A. J. Carty,
K. W. Feindel, G. M. Bernard:
Phosphorus Chemical Shift Tensors of Phosphido Ligands in Ruthenium Carbonyl
Compounds: 31P NMR Spectroscopy of Single-Crystal and Powder Samples and ab initio Calculations.
J. Am. Chem. Soc. 2002, 124, 1541-1552
C. Nachtigal, S. Al-Gharabli, K. Eichele, E. Lindner, H. A. Mayer:
Structural Studies of an Array of Mixed Diamine Phosphine Ruthenium(II) Complexes
Organometallics 2002, 21, 105-112
--- 2001 --- | [UP] |
D. L. Bryce, G. M. Bernard, M. Gee, M. D. Lumsden, K. Eichele, R. E. Wasylishen:
Practical Aspects of Modern Routine Solid-State Multinuclear Magnetic Resonance Spectroscopy:
One-Dimensional Experiments.
Can. J. Anal. Sci. Spectrosc. 2001, 46, 46-82.
B. Thomas, S. Paasch, S. Steuernagel, K. Eichele:
Residual 31P, 35,37Cl Dipolar Coupling in 31P MAS Spectra of
Chlorocyclophosphazenes.
Solid State Nucl. Magn. Reson. 2001, 20, 108-117.
N. Kuhn, K. Eichele, M. Walker:
Synthesis and Structure of 1,3-Diisopropyl-4,5-dimethylimidazolium-2-sulfonate:
A Carbene Adduct of Sulfur Trioxide.
Z. Anorg. Allg. Chem. 2001, 627, 2565-2567.
--- 2000 --- | [UP] |
S. Schweizer, K. Eichele, H. P. T. Ammon, H. Safayhi:
3-Acetoxy Group of Genuine AKBA (Acetyl-11-keto-b-boswellic Acid) is
a-Configurated.
Planta Medica 2000, 66, 781-782.
G. M. Bernard, K. Eichele, G. Wu, C. Kirby, R. E. Wasylishen:
Nuclear Magnetic Shielding Tensors for the Carbon, Nitrogen and Selenium Nuclei of
Selenocyanates—A Combined Experimental and Theoretical Approach.
Can. J. Chem. 2000, 78, 614-625.
E. Lindner, J. Wald, K. Eichele, R. Fawzi:
Synthesis, structure, and reactivity of ruthenium(II) complexes with a hemilabile
tetradentate etherdiphosphine ligand.
J. Organomet. Chem. 2000, 601, 220-225.
M. Gee, R. E. Wasylishen, K. Eichele, J. F. Britten:
Phosphorus Chemical Shift Tensors for Tetramethyldiphosphine Disulfide - A
31P Single-Crystal NMR, Dipolar-Chemical Shift NMR and Ab Initio Molecular Orbital Study.
J. Phys. Chem. A 2000, 104, 4598-4605.
M. Gee, R. E. Wasylishen, K. Eichele, G. Wu, T. S. Cameron, F. Mathey, F. Laporte:
Characterization of Phosphorus Chemical Shielding Tensors in a Phosphole Tetramer:
A Combined Experimental and Theoretical Study.
Can. J. Chem. 2000, 78, 118-127.
--- 1999 --- | [UP] |
K. Eichele, G. Ossenkamp, R. E. Wasylishen, T. S. Cameron, J. F. Britten:
Phosphorus-31 Solid-State NMR Studies of Homonuclear Spin Pairs in Molybdenum Phosphine
Complexes: Single-Crystal, Dipolar-Chemical Shift, Rotational-Resonance and 2D Spin-Echo
NMR Experiments
Inorg. Chem. 1999, 38, 639-651.
--- 1997 --- | [UP] |
K. Eichele, R. E. Wasylishen, J. H. Nelson:
Solid-State 95Mo NMR Studies of Some Prototypal Molybdenum Compounds: Sodium
Molybdate Dihydrate, Hexacarbonylmolybdenum, and Pentacarbonyl Phosphine
Molybdenum (0) Complexes.
J. Phys. Chem. A 1997, 101, 5463-5468.
K. Eichele, R.E. Wasylishen, K. Maitra, J.H. Nelson, J.F. Britten:
Single-Crystal 31P NMR and X-ray Diffraction Study of a Molybdenum Phosphine
Complex: (5-Methyldibenzophosphole)pentacarbonylmolybdenum(0).
Inorg. Chem. 1997, 36, 3539-3544.
K. Eichele, J.C.C. Chan, R.E. Wasylishen, J.F. Britten:
Single-Crystal Cobalt-59 NMR Study of Tris(2,4-pentanedionato-O,O') Cobalt(III).
J. Phys. Chem. A 1997, 101, 5423-5430.
S. Kroeker, K. Eichele, R.E. Wasylishen, J.F. Britten:
Cesium-133 NMR Study of CsCd(SCN)3: Relative Orientation of the Chemical Shift and
Electric Field Gradient Tensors.
J. Phys. Chem. B 1997, 101, 3727-3733.
--- 1996 --- | [UP] |
K.V. Ramanathan, N. Suryaprakash, C.L. Khetrapal, E.D. Becker, K. Eichele and R.E. Wasylishen:
13C MAS NMR Spectra of cis,cis-Mucononitrile in Liquid Crystalline Media and the Solid
State - Orientation of the Carbon Chemical Shift Tensors
J. Magn. Reson. Ser. A 1996, 123, 196-200.
K. Eichele, R.E. Wasylishen, R.W. Schurko, N. Burford, and W.A. Whitla:
An Unusually Large Value of 1J(31P,31P) for a Solid
Triphenyphoshine Phoshadiazonium Cationic Complex: Determination of the Sign of J from 2D Spin-Echo
Experiments
Can. J. Chem. 1996, 74, 2362-2377.
N. Burford, T.S. Cameron, J.A.C. Clyburne, K. Eichele, K.N. Robertson, S. Sereda, R.E. Wasylishen and W.A. Whitla:
Nucleophilic Addition of CH, NH, and OH Bonds to the Phosphadiazonium Cation and Interpretation of 31P
Chemical Shifts at Dicoordinate Phosphorus Centers.
Inorg. Chem. 1996, 35, 5460-5467.
K. Eichele, R.E. Wasylishen, J.M. Kessler, L. Solujic and J.H. Nelson:
Phosphorus Chemical Shift Tensors of Phosphole Derivatives Determined by 31P NMR Spectroscopy of Powder
Samples.
Inorg. Chem. 1996, 35, 3904-3912.
W.L. Wilson, J. Fischer, R.E. Wasylishen, K. Eichele, V.J. Catalano, J.H. Frederick and J.H. Nelson:
Thermal Coupling Reactions of 1-Phenyl-3,4-dimethylphosphole within the Coordination Sphere of Palladium (II).
Inorg. Chem. 1996, 35, 1486-1496.
I.V. Kourkine, M.B. Chapman, D.S. Glueck, K. Eichele, R.E. Wasylishen, G.P.A. Yap, L.M. Liable-Sands and A.L. Rheingold:
Synthesis and Ligand Substitution Reactions of a Mesitylphosphido-Bridged Platinum(II) Dimer.
Inorg. Chem. 1996, 35, 1478-1485.
--- 1995 --- | [UP] |
G. Wu, M.D. Lumsden, G.C. Ossenkamp, K. Eichele and R.E. Wasylishen:
Carbonyl carbon chemical shift tensors for a typical aryl aldehyde and formaldehyde. NMR studies of the isolated 13C-2H spin pair of 3,4-dibenzyloxybenaldehyde-13Ca,2Ha.
J. Phys. Chem. 1995, 99, 15806-15813.
K. Eichele, R. E. Wasylishen, J. F. Corrigan, N. J. Taylor, A. J. Carty:
Phosphorus-31 Chemical Shift Tensors of Phosphinidene Ligands in Ruthenium Carbonyl Cluster Compounds: A 31P Single-Crystal and CP/MAS NMR Study.
J. Am. Chem. Soc. 1995, 117, 6961-6969.
K. Eichele, S. Kroeker, G. Wu, R. E. Wasylishen:
Set-up Samples for 199Hg CP/MAS NMR Spectroscopy.
Solid State Nucl. Magn. Reson. 1995, 4,
295-300.
K. Eichele, R. E. Wasylishen, J. S. Grossert, A. C. Olivieri:
The Influence of Chlorine-Carbon Dipolar and Indirect Spin-Spin Interactions on High-Resolution Carbon-13 NMR Spectra of Chloroketosulfones in the Solid State.
J. Phys. Chem. 1995, 99, 10110-10113.
K. Eichele, G. Wu, R. E. Wasylishen, J. F. Britten:
Phosphorus-31 NMR Studies of Solid Tetraethyldiphosphine Disulfide.
A Reinvestigation of the 31P,31P Spin-Spin Coupling Tensor.
J. Phys. Chem. 1995, 99, 1030-1037.
--- 1994 --- | [UP] |
G. Wu, K. Eichele, R. E. Wasylishen:
Magic-Angle Spinning Frequency Dependent NMR Spectra Arising from
a Pair of Crystallographically Equivalent Phosphorus Nuclei.
In: "Phosphorus-31 NMR Spectral Properties in Compound Characterization
and Structural Analysis"; L. D. Quin, J. G. Verkade (Eds.);
VCH Publishers,
1994, pp 441-450.
M. D. Lumsden, K. Eichele, R. E. Wasylishen, T. S. Cameron,
J. F. Britten:
Determination of a 199Hg-31P Indirect Spin-Spin Coupling Tensor
via Single-Crystal Phosphorus NMR Spectroscopy.
J. Am. Chem. Soc. 1994, 116,
11129-11136.
K. Eichele, R. E. Wasylishen:
High-Resolution 113Cd CP/MAS NMR Studies of Cadmium Thiocyanate
Coordination Compounds. Direct Observation of 113Cd,14N Spin-Spin
Coupling Constants in the Solid State.
Inorg. Chem. 1994, 33, 2766-2773.
K. Eichele, R. E. Wasylishen:
A 31P NMR Study of Powder and Single-Crystal Samples of Ammonium
Dihydrogen Phosphate: The Effect of Homonuclear Dipolar Coupling.
J. Phys. Chem. 1994, 98, 3108-3113.
M. D. Lumsden, R. E. Wasylishen, K. Eichele, M. Schindler,
G. H. Penner, W. P. Power, R. D. Curtis:
The Carbonyl Carbon and Nitrogen Chemical Shift Tensors of the
Amide Fragment of Acetanilide and N-Methylacetanilide.
J. Am. Chem. Soc. 1994, 116, 1403-1413.
Looking for information on acetanilide? Check out my "NMR of acetanilide" page!
R. E. Wasylishen, K. C. Wright, K. Eichele, T. S. Cameron:
Characterization of the J(115In,31P) Tensor for a 1:1 Adduct of
Indium Tribromide and a Triarylphosphine.
Inorg. Chem. 1994, 33, 407-408.
K. Eichele, R. E. Wasylishen:
The Dipolar Splitting Ratio Method - A Convenient Approach to the
Analysis of Dipolar-Chemical Shift NMR Spectra of Static Powder
Samples.
J. Magn. Reson. A 1994, 106, 46-56.
--- 1993 --- | [UP] |
K. L. Moran, T. E. Grier, W. T. A. Harrison, G. D. Stucky, H. Eckert,
K. Eichele, R. E. Wasylishen:
Synthesis and Characterization of Mixed ZnSe/GaP Semiconductor
Species Included in the Sodalite Structure.
J. Am. Chem. Soc. 1993, 115,
10553-10558.
K. Eichele, M. D. Lumsden, R. E. Wasylishen:
Nitrogen-14 Coupled Dipolar-Chemical Shift 13C NMR Spectra of the
Amide Fragment of Peptides in the Solid State.
J. Phys. Chem. 1993, 97, 8909-8916.
K. Eichele, R. E. Wasylishen, J. F. Corrigan, S. Doherty, Y. Sun,
A. J. Carty:
Observations of 1J(P,Ru) in 31P CP/MAS NMR Spectra of Solid
Ruthenium Compounds.
Inorg. Chem. 1993, 32, 121-123.
K. Eichele, G. Wu, R. E. Wasylishen:
Unusual "AB" Spectra in High-Resolution Magic-Angle Spinning
NMR Studies of Solids.
J. Magn. Reson. 1993, A101, 157-161.
K. Eichele, R. E. Wasylishen:
Experimental Characterization of 31P Chemical Shift Tensors in
Phosphine Derivatives.
In: "Nuclear Magnetic Shieldings and Molecular Structure";
J. A. Tossell (Ed.); NATO ASI Series Vol. 386C, p 563,
Kluwer Academic Publishers, Dordrecht 1993.
R. E. Wasylishen, R. D. Curtis, K. Eichele, M. D. Lumsden,
G. H. Penner, W. P. Power, G. Wu:
Applications of Dipolar NMR Spectroscopy in Characterizing
Nitrogen and Phosphorus Shielding Tensors.
In: "Nuclear Magnetic Shieldings and Molecular Structure";
J. A. Tossell (Ed.); NATO ASI Series Vol. 386C, pp 297-314,
Kluwer Academic Publishers, Dordrecht 1993.
--- 1992 --- | [UP] |
K. Eichele, R. E. Wasylishen:
Indirect 113Cd,14N Spin-Spin Coupling Constants as a Structural
Probe of Solid Cadmium Thiocyanate Complexes.
Angew. Chem. 1992, 104, 1263-1265;
Angew. Chem., Int. Ed. Engl. 1992, 31, 1222-1224.
K. Eichele, R. E. Wasylishen:
Observation of nitrogen-14, carbon-13 indirect spin-spin coupling
in high-resolution 13C CP/MAS spectra of solids.
Solid State Nucl. Magn. Reson. 1992, 1, 159-163.
E. Lindner, R. Fawzi, H. A. Mayer, K. Eichele, W. Hiller:
Effect of Ring Size on NMR Parameters: Cyclic Bisphosphine Complexes
of Molybdenum, Tungsten, and Platinum. Bond Angle Dependence of Metal
Shieldings, Metal-Phosphorus Coupling Constants, and the 31P Chemical
Shift Anisotropy in the Solid State.
Organometallics 1992, 11, 1033-1043.
--- 1991 --- | [UP] |
K. Eichele:
Beziehungen zwischen Struktur- und NMR-Parametern von Phosphor-
Verbindungen in Loesung und im Festkoerper.
Ph. D. Thesis, University of Tuebingen 1991.
E. Lindner, R. Fawzi, H. A. Mayer, K. Eichele, K. Pohmer:
Phosphorus-31 Solid-State NMR Studies of Cyclic and Acyclic
Phosphine-Metal Complexes. Determination of Chemical Shift Anisotropy,
Scalar Coupling 1J(M-P) (M = 55Mn, 95/97Mo, 183W), and 55Mn
Quadrupolar Coupling Constants.
Inorg. Chem. 1991, 30, 1102-1107.
--- 1990 --- | [UP] |
E. Lindner, M. Pabel, K. Eichele:
Synthese alkylenverbrueckter Metallkomplexe nach der kationischen
Alkylierung mit Alkandiylbis(trifluormethansulfonaten).
J. Organomet. Chem. 1990, 386, 187-194.
E. Lindner, R. Fawzi, H. A. Mayer, K. Eichele, K. Pohmer:
Darstellung und Eigenschaften von und Reaktionen mit metallhaltigen
Heterocyclen. LXX. Untersuchungen ueber den Zusammenhang zwischen
Konformation und chemischer Verschiebung in
Phosphametallacycloalkanen.
J. Organomet. Chem. 1990, 386, 63-77.