Klaus Eichele:
Publications

Last modified: 18.02.2002

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Contents [2002] [2001] [2000] [1999] [1997] [1996] [1995] [1994] [1993] [1992] [1991] [1990]

    --- 2002 --- [UP]

  1. K. Eichele, R. E. Wasylishen, J. F. Corrigan, N. J. Taylor, A. J. Carty, K. W. Feindel, G. M. Bernard:
    Phosphorus Chemical Shift Tensors of Phosphido Ligands in Ruthenium Carbonyl Compounds: 31P NMR Spectroscopy of Single-Crystal and Powder Samples and ab initio Calculations.
    J. Am. Chem. Soc. 2002, 124, 1541-1552

  2. C. Nachtigal, S. Al-Gharabli, K. Eichele, E. Lindner, H. A. Mayer:
    Structural Studies of an Array of Mixed Diamine Phosphine Ruthenium(II) Complexes
    Organometallics 2002, 21, 105-112

  3. --- 2001 --- [UP]

  4. D. L. Bryce, G. M. Bernard, M. Gee, M. D. Lumsden, K. Eichele, R. E. Wasylishen:
    Practical Aspects of Modern Routine Solid-State Multinuclear Magnetic Resonance Spectroscopy: One-Dimensional Experiments.
    Can. J. Anal. Sci. Spectrosc. 2001, 46, 46-82.

  5. B. Thomas, S. Paasch, S. Steuernagel, K. Eichele:
    Residual 31P, 35,37Cl Dipolar Coupling in 31P MAS Spectra of Chlorocyclophosphazenes.
    Solid State Nucl. Magn. Reson. 2001, 20, 108-117.

  6. N. Kuhn, K. Eichele, M. Walker:
    Synthesis and Structure of 1,3-Diisopropyl-4,5-dimethylimidazolium-2-sulfonate: A Carbene Adduct of Sulfur Trioxide.
    Z. Anorg. Allg. Chem. 2001, 627, 2565-2567.

  7. --- 2000 --- [UP]

  8. S. Schweizer, K. Eichele, H. P. T. Ammon, H. Safayhi:
    3-Acetoxy Group of Genuine AKBA (Acetyl-11-keto-b-boswellic Acid) is a-Configurated.
    Planta Medica 2000, 66, 781-782.

  9. G. M. Bernard, K. Eichele, G. Wu, C. Kirby, R. E. Wasylishen:
    Nuclear Magnetic Shielding Tensors for the Carbon, Nitrogen and Selenium Nuclei of Selenocyanates—A Combined Experimental and Theoretical Approach.
    Can. J. Chem. 2000, 78, 614-625.

  10. E. Lindner, J. Wald, K. Eichele, R. Fawzi:
    Synthesis, structure, and reactivity of ruthenium(II) complexes with a hemilabile tetradentate etherdiphosphine ligand.
    J. Organomet. Chem. 2000, 601, 220-225.

  11. M. Gee, R. E. Wasylishen, K. Eichele, J. F. Britten:
    Phosphorus Chemical Shift Tensors for Tetramethyldiphosphine Disulfide - A 31P Single-Crystal NMR, Dipolar-Chemical Shift NMR and Ab Initio Molecular Orbital Study.
    J. Phys. Chem. A 2000, 104, 4598-4605.

  12. M. Gee, R. E. Wasylishen, K. Eichele, G. Wu, T. S. Cameron, F. Mathey, F. Laporte:
    Characterization of Phosphorus Chemical Shielding Tensors in a Phosphole Tetramer: A Combined Experimental and Theoretical Study.
    Can. J. Chem. 2000, 78, 118-127.

    --- 1999 --- [UP]

  13. K. Eichele, G. Ossenkamp, R. E. Wasylishen, T. S. Cameron, J. F. Britten:
    Phosphorus-31 Solid-State NMR Studies of Homonuclear Spin Pairs in Molybdenum Phosphine Complexes: Single-Crystal, Dipolar-Chemical Shift, Rotational-Resonance and 2D Spin-Echo NMR Experiments
    Inorg. Chem. 1999, 38, 639-651.

    --- 1997 --- [UP]

  14. K. Eichele, R. E. Wasylishen, J. H. Nelson:
    Solid-State 95Mo NMR Studies of Some Prototypal Molybdenum Compounds: Sodium Molybdate Dihydrate, Hexacarbonylmolybdenum, and Pentacarbonyl Phosphine Molybdenum (0) Complexes.
    J. Phys. Chem. A 1997, 101, 5463-5468.

  15. K. Eichele, R.E. Wasylishen, K. Maitra, J.H. Nelson, J.F. Britten:
    Single-Crystal 31P NMR and X-ray Diffraction Study of a Molybdenum Phosphine Complex: (5-Methyldibenzophosphole)pentacarbonylmolybdenum(0).
    Inorg. Chem. 1997, 36, 3539-3544.

  16. K. Eichele, J.C.C. Chan, R.E. Wasylishen, J.F. Britten:
    Single-Crystal Cobalt-59 NMR Study of Tris(2,4-pentanedionato-O,O') Cobalt(III).
    J. Phys. Chem. A 1997, 101, 5423-5430.

  17. S. Kroeker, K. Eichele, R.E. Wasylishen, J.F. Britten:
    Cesium-133 NMR Study of CsCd(SCN)3: Relative Orientation of the Chemical Shift and Electric Field Gradient Tensors.
    J. Phys. Chem. B 1997, 101, 3727-3733.

    --- 1996 --- [UP]

  18. K.V. Ramanathan, N. Suryaprakash, C.L. Khetrapal, E.D. Becker, K. Eichele and R.E. Wasylishen:
    13C MAS NMR Spectra of cis,cis-Mucononitrile in Liquid Crystalline Media and the Solid State - Orientation of the Carbon Chemical Shift Tensors
    J. Magn. Reson. Ser. A 1996, 123, 196-200.

  19. K. Eichele, R.E. Wasylishen, R.W. Schurko, N. Burford, and W.A. Whitla:
    An Unusually Large Value of 1J(31P,31P) for a Solid Triphenyphoshine Phoshadiazonium Cationic Complex: Determination of the Sign of J from 2D Spin-Echo Experiments
    Can. J. Chem. 1996, 74, 2362-2377.

  20. N. Burford, T.S. Cameron, J.A.C. Clyburne, K. Eichele, K.N. Robertson, S. Sereda, R.E. Wasylishen and W.A. Whitla:
    Nucleophilic Addition of CH, NH, and OH Bonds to the Phosphadiazonium Cation and Interpretation of 31P Chemical Shifts at Dicoordinate Phosphorus Centers.
    Inorg. Chem. 1996, 35, 5460-5467.

  21. K. Eichele, R.E. Wasylishen, J.M. Kessler, L. Solujic and J.H. Nelson:
    Phosphorus Chemical Shift Tensors of Phosphole Derivatives Determined by 31P NMR Spectroscopy of Powder Samples.
    Inorg. Chem. 1996, 35, 3904-3912.

  22. W.L. Wilson, J. Fischer, R.E. Wasylishen, K. Eichele, V.J. Catalano, J.H. Frederick and J.H. Nelson:
    Thermal Coupling Reactions of 1-Phenyl-3,4-dimethylphosphole within the Coordination Sphere of Palladium (II).
    Inorg. Chem. 1996, 35, 1486-1496.

  23. I.V. Kourkine, M.B. Chapman, D.S. Glueck, K. Eichele, R.E. Wasylishen, G.P.A. Yap, L.M. Liable-Sands and A.L. Rheingold:
    Synthesis and Ligand Substitution Reactions of a Mesitylphosphido-Bridged Platinum(II) Dimer.
    Inorg. Chem. 1996, 35, 1478-1485.

    --- 1995 --- [UP]

  24. G. Wu, M.D. Lumsden, G.C. Ossenkamp, K. Eichele and R.E. Wasylishen:
    Carbonyl carbon chemical shift tensors for a typical aryl aldehyde and formaldehyde. NMR studies of the isolated 13C-2H spin pair of 3,4-dibenzyloxybenaldehyde-13Ca,2Ha.
    J. Phys. Chem. 1995, 99, 15806-15813.

  25. K. Eichele, R. E. Wasylishen, J. F. Corrigan, N. J. Taylor, A. J. Carty:
    Phosphorus-31 Chemical Shift Tensors of Phosphinidene Ligands in Ruthenium Carbonyl Cluster Compounds: A 31P Single-Crystal and CP/MAS NMR Study.
    J. Am. Chem. Soc. 1995, 117, 6961-6969.

  26. K. Eichele, S. Kroeker, G. Wu, R. E. Wasylishen:
    Set-up Samples for 199Hg CP/MAS NMR Spectroscopy.
    Solid State Nucl. Magn. Reson. 1995, 4, 295-300.

  27. K. Eichele, R. E. Wasylishen, J. S. Grossert, A. C. Olivieri:
    The Influence of Chlorine-Carbon Dipolar and Indirect Spin-Spin Interactions on High-Resolution Carbon-13 NMR Spectra of Chloroketosulfones in the Solid State.
    J. Phys. Chem. 1995, 99, 10110-10113.

  28. K. Eichele, G. Wu, R. E. Wasylishen, J. F. Britten:
    Phosphorus-31 NMR Studies of Solid Tetraethyldiphosphine Disulfide. A Reinvestigation of the 31P,31P Spin-Spin Coupling Tensor.
    J. Phys. Chem. 1995, 99, 1030-1037.

    --- 1994 --- [UP]

  29. G. Wu, K. Eichele, R. E. Wasylishen:
    Magic-Angle Spinning Frequency Dependent NMR Spectra Arising from a Pair of Crystallographically Equivalent Phosphorus Nuclei.
    In: "Phosphorus-31 NMR Spectral Properties in Compound Characterization and Structural Analysis"; L. D. Quin, J. G. Verkade (Eds.); VCH Publishers, 1994, pp 441-450.

  30. M. D. Lumsden, K. Eichele, R. E. Wasylishen, T. S. Cameron, J. F. Britten:
    Determination of a 199Hg-31P Indirect Spin-Spin Coupling Tensor via Single-Crystal Phosphorus NMR Spectroscopy.
    J. Am. Chem. Soc. 1994, 116, 11129-11136.

  31. K. Eichele, R. E. Wasylishen:
    High-Resolution 113Cd CP/MAS NMR Studies of Cadmium Thiocyanate Coordination Compounds. Direct Observation of 113Cd,14N Spin-Spin Coupling Constants in the Solid State.
    Inorg. Chem. 1994, 33, 2766-2773.

  32. K. Eichele, R. E. Wasylishen:
    A 31P NMR Study of Powder and Single-Crystal Samples of Ammonium Dihydrogen Phosphate: The Effect of Homonuclear Dipolar Coupling.
    J. Phys. Chem. 1994, 98, 3108-3113.

  33. M. D. Lumsden, R. E. Wasylishen, K. Eichele, M. Schindler, G. H. Penner, W. P. Power, R. D. Curtis:
    The Carbonyl Carbon and Nitrogen Chemical Shift Tensors of the Amide Fragment of Acetanilide and N-Methylacetanilide.
    J. Am. Chem. Soc. 1994, 116, 1403-1413.
     
     
    Looking for information on acetanilide? Check out my "NMR of acetanilide" page!

     

  34. R. E. Wasylishen, K. C. Wright, K. Eichele, T. S. Cameron:
    Characterization of the J(115In,31P) Tensor for a 1:1 Adduct of Indium Tribromide and a Triarylphosphine.
    Inorg. Chem. 1994, 33, 407-408.

  35. K. Eichele, R. E. Wasylishen:
    The Dipolar Splitting Ratio Method - A Convenient Approach to the Analysis of Dipolar-Chemical Shift NMR Spectra of Static Powder Samples.
    J. Magn. Reson. A 1994, 106, 46-56.

    --- 1993 --- [UP]

  36. K. L. Moran, T. E. Grier, W. T. A. Harrison, G. D. Stucky, H. Eckert, K. Eichele, R. E. Wasylishen:
    Synthesis and Characterization of Mixed ZnSe/GaP Semiconductor Species Included in the Sodalite Structure.
    J. Am. Chem. Soc. 1993, 115, 10553-10558.

  37. K. Eichele, M. D. Lumsden, R. E. Wasylishen:
    Nitrogen-14 Coupled Dipolar-Chemical Shift 13C NMR Spectra of the Amide Fragment of Peptides in the Solid State.
    J. Phys. Chem. 1993, 97, 8909-8916.

  38. K. Eichele, R. E. Wasylishen, J. F. Corrigan, S. Doherty, Y. Sun, A. J. Carty:
    Observations of 1J(P,Ru) in 31P CP/MAS NMR Spectra of Solid Ruthenium Compounds.
    Inorg. Chem. 1993, 32, 121-123.

  39. K. Eichele, G. Wu, R. E. Wasylishen:
    Unusual "AB" Spectra in High-Resolution Magic-Angle Spinning NMR Studies of Solids.
    J. Magn. Reson. 1993, A101, 157-161.

  40. K. Eichele, R. E. Wasylishen:
    Experimental Characterization of 31P Chemical Shift Tensors in Phosphine Derivatives.
    In: "Nuclear Magnetic Shieldings and Molecular Structure"; J. A. Tossell (Ed.); NATO ASI Series Vol. 386C, p 563, Kluwer Academic Publishers, Dordrecht 1993.

  41. R. E. Wasylishen, R. D. Curtis, K. Eichele, M. D. Lumsden, G. H. Penner, W. P. Power, G. Wu:
    Applications of Dipolar NMR Spectroscopy in Characterizing Nitrogen and Phosphorus Shielding Tensors.
    In: "Nuclear Magnetic Shieldings and Molecular Structure"; J. A. Tossell (Ed.); NATO ASI Series Vol. 386C, pp 297-314, Kluwer Academic Publishers, Dordrecht 1993.

    --- 1992 --- [UP]

  42. K. Eichele, R. E. Wasylishen:
    Indirect 113Cd,14N Spin-Spin Coupling Constants as a Structural Probe of Solid Cadmium Thiocyanate Complexes.
    Angew. Chem. 1992, 104, 1263-1265;
    Angew. Chem., Int. Ed. Engl. 1992, 31, 1222-1224.

  43. K. Eichele, R. E. Wasylishen:
    Observation of nitrogen-14, carbon-13 indirect spin-spin coupling in high-resolution 13C CP/MAS spectra of solids.
    Solid State Nucl. Magn. Reson. 1992, 1, 159-163.

  44. E. Lindner, R. Fawzi, H. A. Mayer, K. Eichele, W. Hiller:
    Effect of Ring Size on NMR Parameters: Cyclic Bisphosphine Complexes of Molybdenum, Tungsten, and Platinum. Bond Angle Dependence of Metal Shieldings, Metal-Phosphorus Coupling Constants, and the 31P Chemical Shift Anisotropy in the Solid State.
    Organometallics 1992, 11, 1033-1043.

    --- 1991 --- [UP]

  45. K. Eichele:
    Beziehungen zwischen Struktur- und NMR-Parametern von Phosphor- Verbindungen in Loesung und im Festkoerper.
    Ph. D. Thesis, University of Tuebingen 1991.

  46. E. Lindner, R. Fawzi, H. A. Mayer, K. Eichele, K. Pohmer:
    Phosphorus-31 Solid-State NMR Studies of Cyclic and Acyclic Phosphine-Metal Complexes. Determination of Chemical Shift Anisotropy, Scalar Coupling 1J(M-P) (M = 55Mn, 95/97Mo, 183W), and 55Mn Quadrupolar Coupling Constants.
    Inorg. Chem. 1991, 30, 1102-1107.

    --- 1990 --- [UP]

  47. E. Lindner, M. Pabel, K. Eichele:
    Synthese alkylenverbrueckter Metallkomplexe nach der kationischen Alkylierung mit Alkandiylbis(trifluormethansulfonaten).
    J. Organomet. Chem. 1990, 386, 187-194.

  48. E. Lindner, R. Fawzi, H. A. Mayer, K. Eichele, K. Pohmer:
    Darstellung und Eigenschaften von und Reaktionen mit metallhaltigen Heterocyclen. LXX. Untersuchungen ueber den Zusammenhang zwischen Konformation und chemischer Verschiebung in Phosphametallacycloalkanen.
    J. Organomet. Chem. 1990, 386, 63-77.


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